Planning (a) and (b) in Chemistry Internal Assessment

The following list of investigation titles is divided into two groups:

  1. experiments suitable for planning (a) and (b)
  2. experiments suitable for planning (b) only.

For each title, a list of the possible variables is included. Experiments suitable for planning (a) have at least two independent variables that could be manipulated during an investigation. The titles are sufficiently specific to give candidates a sense of direction, but they are not sufficiently specific to serve as a research question. Candidates will have to modify the statement to make it more specific and focused. In most cases, this will involve indicating the variable(s) chosen for investigation. Where the title completely specifies the problem, and only one or no variables can be manipulated, the experiment is listed for planning (b) only. If the experiment is to be used to assess planning (a), candidates should not be given information about the possible variables, since one aspect of planning (a) concerns the candidate's ability to select the relevant variables without help from the teacher.

Variables are things we measure, control or manipulate in an investigation. Independent variables are those that are manipulated, whereas dependent variables are measured or registered. The variable that is selected for manipulation is independent, the variable that depends on the manipulation is dependent. Thus, in a calorimetry investigation, where a candidate measures the temperature every 30 seconds, time is the independent variable, and temperature is the dependent variable. Similarly, in a rate investigation, where the candidate measures the times taken to collect certain volumes of gas, volume is independent, and time is dependent.

Investigations Suitable for Planning (a) and (b)

Click here for a description of the planning criteria.

1. Investigate the volume of a drop

Dependent:

Volume or mass of liquid

Independent:

Nature of liquid, includes mass, density, viscosity (these cannot be separated)

 

Temperature

 

Material of dropper

 

Size of opening

 

Angle of delivery

 

Speed of delivery

 

Height of water column

 

Pressure (external)

Note: This is a very simple experiment suitable as a first exposure to practise the skills associated with planning (a) and (b). Any of the first seven independent variables can be investigated.

2. Investigate the height of a liquid in a capillary tube

Dependent:

Height of liquid

Independent:

Nature of liquid

 

Diameter of tube

 

Material of tube

 

Angle of tube

 

Temperature

 

Overall length of tube

 

Depth of capillary tube in the liquid

Note: Suitable for practice for planning (a) and (b). Any of the independent variables could be tested.

3. Investigate factors influencing the solubility of salts

Dependent:

Mass of solute

Independent:

Volume or mass of water

 

Temperature

 

Anion

 

Cation

 

Relation of charges of the ions

Note: Candidates will probably control the first independent variable and can manipulate any of the last three.

4. Investigate the catalysed decomposition of hydrogen peroxide

Dependent:

Some measure of change of concentration of a reactant or product (volume of gas, decrease in mass, or concentration of hydrogen peroxide)

Independent:

Relative quantity of catalyst

 

Concentration of hydrogen peroxide

 

Other transition metal oxides

 

Other manganese compounds

 

Oxides or metals

 

State of division

 

Heterogeneous or homogeneous catalysis

 

Temperature

Note: Temperature will probably be controlled. Any of the other independent variables can be investigated.

5. Investigate exposure to radiation

Dependent:

Counts per unit time

Independent:

Type of radiation

 

Type of barrier

 

Thickness of barrier

 

Distance between source and detector

 

Strength of magnetic field

 

Angle between detector and source

 

Time of counting

 

Temperature

Note: Any of the independent variables can be easily manipulated, apart from temperature which will probably be controlled.

6. Investigate the rate of electroplating a metal

Dependent:

Quantity of metal deposited

Independent:

Time

 

Temperature

 

Concentration of solution

 

Identity of metal

 

Size of electrode

 

Voltage

 

Current

Note: Any of the independent variables could be investigated.

7. Investigate the equilibrium reaction between an alkanoic acid and an alkanol

Dependent:

Quantity of ester (or change in concentration of acid or alkanol)

Independent:

Initial concentrations of acid and alkanol

 

Time elapsed

 

Temperature

 

Nature of acid

 

Nature of alkanol

 

Method of measurement

Note: Any of the first five independent variables could be manipulated, but this presents a difficult and time-consuming experiment. It would be easier for the teacher to direct the candidates to measure the amounts of acid, and to grade this for planning (b) only.

8. Investigate the effect of acid rain on building materials

Dependent:

Effect on material

Independent:

Type of material

 

Time of exposure

 

Surface area exposed

 

Method of measurement

 

Temperature

 

Nature of acid

 

Concentration of acid

 

Nature of exposure

Note: Any of the independent variables could be investigated.

9. Investigate the conditions affecting the rate of escape of carbon dioxide from soda water

Dependent:

Quantity of gas released

Independent:

Time

 

Temperature

 

Amount of soda water

 

Depth of soda water

 

Surface area of soda water

 

Material of container

 

Extent of agitation of the soda water

 

Pressure

Note: Any of the first seven independent variables could be investigated.

10. Investigate the amount of a solid that will dissolve in a solvent

Dependent:

Quantity of solid

Independent:

Nature of solid

 

Quantity of solvent

 

Nature of solvent

 

Time

 

Order of addition

 

Temperature

 

Stirring

 

State of division

Note: Any of the independent variables could be investigated. The effect of the last three is probably known in advance.

11. Investigate the factors influencing the voltage of an electrochemical cell

Dependent:

Voltage

Independent:

Size of electrodes

 

Distance between electrodes

 

Nature of electrodes

 

Nature of solution

 

Concentration of solution

 

Method of measurement

 

Nature of ion transfer (salt bridge)

Note: Any of the first five independent variables could be investigated.

12. Investigate the factors affecting retention in paper chromatography

Dependent:

Distance travelled by spot

Independent:

Thickness of paper

 

Nature of paper

 

Eluting solvent

 

Size of spot

 

Concentration of solute

 

Distance solvent travels

 

Nature of solute

 

Temperature

Note: Any of the first six independent variables could be manipulated.

13. Investigate testing the energy from liquid fuels

Dependent:

Temperature change of water

Independent:

Construction of calorimeter (including nature of water container, amount and location of insulation, supply of oxygen)

 

Type of fuel

 

Amount of fuel/time of burning

 

Amount of water

 

Distance of flame from calorimeter

Note: The first set of independent variables will be manipulated, and perhaps also the type of fuel. The last three independent variables will need to be controlled.

14. Investigate the factors affecting the rate of a reaction

Dependent:

Change in concentration

Independent:

Nature of reaction

 

Concentration of reagents

 

Total volume

 

Temperature

 

State of division (only for heterogeneous reaction)

 

Catalysis

Note: Once a candidate chooses a reaction, at least two other independent variables could be manipulated.

15. Determine a property of a gas

Dependent:

Measurements

Independent:

Property investigated

 

Temperature

 

Volume

 

Pressure

 

Amount of gas

Note: The property chosen should be one where a variable can be changed. Candidates should have to devise their own methods, rather than following familiar techniques.

16. Investigate the factors that affect the rate of the reaction between sodium thiosulfate and hydrochloric acid

Dependent:

Time for visual change

Independent:

Total volume of solution

 

Concentration of sodium thiosulfate

 

Concentration of hydrochloric acid

 

Temperature

Note: Several variables could be manipulated. This is a very simple variation on investigation 14 (above).

Investigations Suitable for Planning (b) Only

1. Investigate reactions of hydrocarbons

Dependent:

Evidence for reaction

Independent:

Temperature

 

Time

 

Light

 

Concentrations

 

Specific substrate

 

Reagent

Note: This investigation has been listed for planning (b) only because the teacher will probably have to give information to the class about the relevant variables. This experiment has been carried out testing the possible reactions of bromine solution and the acid-catalysed addition of water to cyclohexane, cyclohexene, chlorobenzene, and methylbenzene. Any of the first four variables could be investigated.

2. Investigate how the densities of specified solutions vary with their concentrations

Dependent:

Mass of solution

Independent:

Concentration of solution

 

Method of dilution

 

Volume of solution

Note: Only concentration of the solution will be varied. The challenge is to keep volumes constant by dilution in a volumetric flask, rather than dilution by adding known volumes of solvent and solution.

3. Determine the molar mass of a gas

Dependent:

Mass

Independent:

Volume

 

Temperature

 

Pressure

Note: Probably no variable will be manipulated.

4. Determine the molar mass of a volatile liquid

Dependent:

Mass

Independent:

Identity of liquid

 

Quantity of liquid

 

Temperature

 

Pressure

Note: Probably no variable will be manipulated.

5. Design a hot or cold pack to specifications

Dependent:

Temperature change

Independent:

Identity of chemical

 

Quantity of chemical

 

Quantity of water

 

Original temperature

Note: This would probably be done by varying the quantity of chemical or water, and keeping other factors constant.

6. Determine the enthalpy of a reaction by a Hess's law relationship

Dependent:

Temperature change

Independent:

Nature of reactions

 

Quantities of reactants

 

Pressure

 

Method of measurement

Note: The independent variables have to be controlled, rather than varied.

7. Determine the order of a reaction with respect to a specified reagent

Dependent:

Change of concentration

Independent:

Total volume of solution

 

Concentration of reagent A

 

Concentration of reagent B

 

Temperature

Note: One concentration can be varied while other factors are kept constant.

8. Investigate the temperature of a Bunsen burner flame

Dependent:

Temperature (relative rather than absolute)

Independent:

Method of measurement

 

Location of measurement

 

Amount of gas

 

Relative amounts of gas and air

Note: Several factors could be varied, but they would be difficult to measure.

9. Investigate the concentration ranges in which starch and iodine react

Dependent:

Evidence for reaction

Independent:

Relative concentrations of starch and iodine

 

Presence of other substances

 

Temperature

 

Time

Note: Candidates are likely to change the first independent variable.

10. Investigate the conditions for glucose oxidase to react with glucose

Dependent:

Measured effect

Independent:

Measurement method

 

Concentration of glucose

 

Time

 

Temperature

 

Quantity of solution

 

Presence of other substances in solution

Note: Candidates are likely to investigate the concentration necessary for reaction.

11. Investigate the relationship between the strength of an egg shell and its composition

Dependent:

Measurement of strength

Independent:

Method of measurement

 

Different eggs

 

Size of sample portion

 

Analysis of composition

Note: Candidates will control variables rather than manipulate them.

12. Investigate the composition of a common substance by acid–base titration

 

Dependent:

Volume of titrant

Independent:

Identity of analyte

 

Quantity of sample

 

Concentration of titrant

 

Indicator

Note: Candidates will control variables and specify their values rather than manipulate them.

 

13. Investigate the composition of a common substance by oxidation–reduction titration

Variables and evaluation are similar to investigation 12 above.

 

14. Investigate how the colour produced by iron(III) and thiocyanate ions varies with concentrations

Dependent:

Absorbance

Independent:

Wavelength

 

Concentration of Fe(III) ions

 

Concentration of thiocyanate ions

 

Identity of complex formed

Note: Candidates will probably vary one concentration or the other, while keeping other
variables constant.

Note: In addition to the candidate work, samples submitted for moderation must include the instructions, written or oral, given to the candidate by the teacher. This vital information is used by moderators to assess whether the experiment, as given, was suitable for assessing the criteria.

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